Si-Al固溶对Ti3AlC2陶瓷300℃干摩擦行为的影响曾庆妍1,2,薛垄琦1,2,3,王传超1,2,王金金1,2,杜乘风1,2,3,余泓1,2(1.西北工业大学凝固技术国家重点实验室,陕西西安710072;2.西北工业大学先进润滑与密封材料研究中心,陕西西安710072;3.西北工业大学伦敦玛丽女王工程学院,陕西西安710072)摘要:利用元素粉体热压烧结工艺制备了具有不同Si固溶含量的系列Ti3Al1-xSixC2(x=0.2、0.4、0.6)陶瓷材料,采用X射线衍射技术及Rietveld结构精修对所得产物的结构及相组成进行了分析,利用共聚焦显微镜、扫描电子显微镜研究了产物的表面形貌和晶粒结构,使用球-盘型摩擦实验机评估了材料的干摩擦行为。结果表明,Si的引入极大细化了Ti3Al1-xSixC2陶瓷的晶粒,并降低其相纯度。随着Si加入量的增加,大量Ti5Si3和TiC杂相出现,Ti3Al1-xSixC2陶瓷的硬度逐步提升。而当Si加入量为0.4时,所得Ti3Al0.6Si0.4C2陶瓷表现出了最低的摩擦系数(COF),为0.27,抗磨减摩效果最好。关键词:MAX陶瓷;固溶;晶粒尺寸;相组成;干摩擦行为中图分类号:TG115.5+8文献标识码:A文章编号:1000-8365(2023)03-0227-06EffectsofSi-AlSolidSolutionontheDrySlidingBehaviorsofTi3AlC2at300℃ZENGQingyan1,2,XUELongqi1,2,3,WANGChuanchao1,2,WANGJinjin1,2,DUChengfeng1,2,3,YUHong1,2(1.StateKeyLaboratoryofSolidificationProcessing,NorthwesternPolytechnicalUniversity,Xi'an710072,China;2.CenterofAdvancedLubricationandSealMaterials,NorthwesternPolytechnicalUniversity,Xi'an710072,China;3.QueenMaryUniversityofLondonEngineeringSchool,NorthwesternPolytechnicalUniversity,Xi'an710072,China)Abstract:Hot-pressingofelementalpowdershasbeenappliedforpreparingaseriesofTi3Al1-xSixC2(x=0.2,0.4,0.6)ceramicswithdifferentSicontents.ThecrystalstructureandphasecompositionoftheproductswerecharacterizedbyX-raydiffractionandRietveldrefinement.Meanwhile,thesurfacemorphologiesandgraindistributionwereanalysedviaconfocalmicroscopyandscanningelectronmicroscopy.Thetribologicalperformanceoftheproductswasevaluatedthroughdryslidingonatribometerwithaball-on-diskconfiguration.Consequently,theadditionofSigreatlyreducesthegrainsizeofTi3Al1-xSixC2,whereasthepurityofthesampledecreasesaswell.ThecontentsofTi5Si3andTiCimpur...