_STP_1473-2006.pdf

STP 1473Beryllium:Sampling and AnalysisDr.Kevin Ashley,editorASTM Stock Number:STP1473ASTM International100 Barr Harbor DrivePO Box C700West Conshohocken,PA 19428-2959Printed in the U.S.A.Library of Congress Cataloging-in-Publication DataSymposium on Beryllium Sampling and Analysis(2005:Reno,Nev.)Beryllium:sampling and analysis/Kevin Ashley.ISBN-13:978-0-8031-3499-7ISBN-10:0-8031-3499-1p.;cm.(STP;1473)Contains papers presented at the Symposium on Beryllium Sampling and Analysis,which washeld in Reno,NV(USA)on 21-22 April,2005.The symposium was sponsored by ASTM International Committee D22 on Air Quality and itsSubcommittee D22.04 on Sampling and Analysis of Workplace Atmospheres,in cooperation with theSampling and Analysis Subcommittee of the Beryllium Health and Safety Committee-Foreword.1.BerylliumAnalysisCongresses.I.Ashley,Kevin.II.ASTM International.Committee D22on Air Quality.III.ASTM International.Subcommittee D22.04 on Sampling and Analysis of Workplace Atmospheres.IV.ASTMInternational.Beryllium Health and Safety Committee.Sampling and Analysis Subcommittee.V.Title.VI.Series:ASTM special technical publication;1473.DNLM:1.Beryllium-isolation&purification-Congresses.2.BerylliumanalysisCongresses.QV 275 S989b 2006QD181.B4S96 2006615.925391dc222006022213Copyright 2006 AMERICAN SOCIETY FOR TESTING AND MATERIALS INTERNATIONAL,West Conshohocken,PA.All rights reserved.This material may not be reproduced or copied,inwhole or in part,in any printed,mechanical,electronic,film,or other distribution and storage media,without the written consent of the publisher.Photocopy RightsAuthorization to photocopy items for internal,personal,or educational classroom use,orthe internal,personal,or educational classroom use of specific clients,is granted by theAmerican Society for Testing and Materials International(ASTM)provided that the appropriatefee is paid to the Copyright Clearance Center,222 Rosewood Drive,Danvers,MA 01923;Tel:978-750-8400;online:http:/ Review PolicyEach paper published in this volume was evaluated by two peer reviewers and at least one editor.The authors addressed all of the reviewers comments to the satisfaction of both the technicaleditor(s)and the ASTM International Committee on Publications.The quality of the papers in this publication reflects not only the obvious efforts of the au-thors and the technical editor(s),but also the work of the peer reviewers.In keeping with long-stand-ing publication practices,ASTM International maintains the anonymity of the peer reviewers.TheASTM International Committee on Publications acknowledges with appreciation their dedication andcontribution of time and effort on behalf of ASTM International.Printed in Lancaster,PAAugustw,2006ForewordThis publication,Beryllium:Sampling and Analysis,contains papers presented at theSymposium on Beryllium Sampling and Analysis,which was held in Reno,NV(USA)on 2122April,2005.The symposium was sponsored by ASTM International Committee D22 on Air Qualityand its Subcommittee D22.04 on Sampling and Analysis of Workplace Atmospheres,in cooperationwith the Sampling and Analysis Subcommittee of the Beryllium Health and Safety Committee.Dr.Kevin Ashley,Centers for Disease Control and Prevention/National Institute for OccupationalSafety and Health,presided as symposium chairman and served as editor of this compilation.Co-chairs of the symposium were Kathryn L.Creek,Los Alamos National Laboratory;David Hamel,Occupational Safety and Health Administration;Michael J.Brisson,Washington Savannah RiverCompany;and Dr.Amy Ekechukwu,Savannah River National Laboratory.Kevin Ashley,Ph.D.CDC/NIOSH,Cincinnati,OHSymposium Chairman and EditoriiiContents ForwardiiiOverviewviiAcknowledgmentsixBERYLLIUMDISEASE EXPOSUREMONITORING ANDSTANDARDIZATIONISSUESOpportunities for Standardization of Beryllium Sampling and AnalysisM.J.BRISSON,A.A.EKECHUKWU,K.ASHLEY,ANDS.D.JAHN3Standard Methods for Beryllium Sampling and Analysis:Availabilities and NeedsK.ASHLEY,M.J.BRISSON,ANDS.D.JAHN15BERYLLIUMEXPOSUREMEASUREMENT ANDREFERENCEMATERIALS NATIONAL ANDINTERNATIONALPERSPECTIVESOpportunities for Development of Reference Materials for BerylliumR.L.WATTERS,JR.,M.D.HOOVER,G.A.DAY,ANDA.B.STEFANIAK29Characteristics of Beryllium Oxide and Beryllium Metal Powders for Use as ReferenceMaterialsA.B.STEFANIAK,M.D.HOOVER,G.A.DAY,A.A.EKECHUKWU,G.E.WHITNEY,C.A.BRINK,ANDR.C.SCRIPSICK47Determination of Beryllium Compounds by NIOSH 7303S.AMER,D.SMIEJA,J.LOUGHRIN,ANDL.REICHMANN62Sampling and Analysis of Beryllium at JET:Policy Cost and ImpactD.CAMPLINGANDB.PATEL68vON-SITEMONITORING FORBERYLLIUM SAMPLING ANDANALYTICALASPECTSUse of Electrically Enhanced Aerosol Plasma Spectroscopy for Real-Time Characterization of Beryllium ParticlesM.-D.CHENG,R.W.SMITHWICK,III,ANDR.HINTON81Development of a New Fluorescence Method for the Detection of Beryllium on SurfacesE.M.MINOGUE,D.S.EHLER,A.K.BURRELL,T.M.MCCLESKEY,ANDT.P.TAYLOR92Interlaboratory Evaluation of a Portable Fluorescence Method for the Measure