ASTM_D_2360_-_04_rus.pdf

1561-2005 I aii (ASTM D 2360-04,IDT)3-2005 1561-2005 665.6.033.25:543.544.3(083.74)71.080.10;71.040.50 06 ID :,.1 2 19 2005.33 3 ASTM D 2360-04 Standard Test Method for trace impurities inmonocyclic aromatic hydrocarbons by gas chromatography(ATM 2360-04 ).:ASTM D (/)001;2(),.ASTM D 16 ,D 16.01 ,.(en).ASTM D,-,.(IDT)4 II 1561-2005 1 .1 2 .1 3.2 4 .2 5 .2 6 .2 7.3 8 .4 9.4 10 .4 11 .4 12.4 13 .6 14 .6 15.7 16 .7 17 .8 III 1561-2005 1)I ii Monocyclic Aromatic Hydrocarbons.Standard test method for trace impurities by gas chromatography 2005-11-01 1 1.1 .1.2 ,()0,001 2,500%(.).1.2.1 .1.3 ,(,)0,001%1,000%(ac.),.1.4 ASTM 29.1.5 .,OSHA,.2 2.1 ASTM2):ASTM D 841 ASTM D 2306 8 ASTM D 3437 ASTM D 3797 -ASTM D 3798 -ASTM D 4492 ASTM D 4790 .ASTM D 5211 -1)D 16 -D 16.01 ,-.1 2004.,2004.1966.2003.,ASTM D 2360-03.2)S www.astm.org serviceastm.org.S S.1 1561-2005 ASTM D 6809 -ASTM E 29 ASTM 260 ASTM 355 ASTM E 691 ASTM 1510 2.2 :S3),29 CFR,1910.1000 1910.1200*3 3.1 3.1.1 ,-ASTM D 4790.4 4.1 ,-.,.,100,00.5 5.1 ,.,.,(),.5.1.1 -,-ASTM D 3797,ASTM D 3798 ASTM D 4492.5.1.2 8-ASTM D 2306.5.2 -100,00.,.6 6.1 .,50%.3)Superintendent of Documents,U.S.Government Printing Office,Washington DC 20402.*11-19-94 ,70 03.06.2003.2 1561-2005 6.2 -,.7 7.1 .,-,1.-,10/-,.7.2:().,-.-1.7.3 .7.4 10,50 500.7.5 50.1 -:,0,25 ,60 ,0,32(),:270 300 :,60 1,10 ,150 ,/5 2,10 -,/1,0 100:1 ,1,0 ,30 145,/20 Carbowax 20,.3 1561-2005 8 8.1 .,4).,.8.2-.,.99,999%.-1 m,0,5 m.-,.8.3 .8.4-,99,999%.8.4.1-99,9%.1,9 -3,8 -5 10 5.-,.-.,-.8.5 .-,-.99%.99%,.8.5.1 .-(),6.9 OSHA,.10 ASTM D 3437.11 ,1.-ASTM E 260,ASTM E 355 ASTM E 1510.12 12.1 -.0,1.2.-,-.,.4),American Chemical Society,Washington,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.4 1561-2005 12.2 (1).-2.Ci=(Di)(Vi)/(Vp)(Dp)(100),(1)Di i(.2);Vi i,;Dp -(.2);Vp -,;i i,%.2 ,%,%-(.8.4.1)-0,857 0,874 0,862 0,863 0,876 0,857 0,714 50,00 10,0 10,0 50,0 50,0 10,0 10,0 99,72 0,020 0,020 0,100 0,100 0,020 0,020 99,72 0,020 0,020 0,101 0,099 0,020 0,017 25.1 10,ASTM-4,1971.12.3 50,00 50,0 50.0,857 0,856,0,100%,(1).12.3.1 ,25.12.4 ,12.3.-1.12.5 ,)()(isisiACCARRF=(2)RRFi i -;i i;S ,;Cs ,%;i i,12.2,%.12.6 0,001.5 1561-2005 1 13 13.1 ,-25.-,12.50,0 -50,50,00 ,.13.2 -.,7.1.13.3 ,.-.().9-,-.9-.13.4 2 ASTM D 841.3 ASTM D 5211.14 14.1 ,)()()(ssiiiACRRFAC=(3)14.2 ,Vi=(Ci)(Ds)/Di,(4)Vi i,%;Di i(.2);Ds .14.3 =100,00 Ct,(5)Ct ,%.6 1561-2005 2 ASTM D 841 3 ASTM D 5211 15 15.1 .15.1.1 0,001%.15.1.2 0,001%0,001%-.15.1.3 0,01%.15.1.4 (GC)0,01%.16 5)16.1.95%,-,-.,.ASTM 691.5)-ASTM.RR:D16-1020.7 1561-2005 16.1.1 3 .16.2.,3.16.3.,-,3.3 ,c ,%:(0,023)0,0067 0,0110 (0,017)0,0041 0,0063-(0,010)0,0038 0,0038-(0,012)0,0031 0,0040-(0,001)0,0003 0,0003 (99,94)0,0160 0,0210 :(2,526)0,150 0,816 (0,649)0,052 0,153 (0,010)0,0007 0,0013 (96,82)0,180 0,819 16.4 .-.17 17.1 ,S D 6809,QA/QC,.8 .02.08.2005 30.09.2005 6084/8.1,39 .-.0,50 .:()02330/0133084 30.04.2004,220113,.,.,3