ICS11.220B41DB37山东省地方标准DB37/T4051—2020中兽药散剂中添加喹乙醇、乙酰甲喹的测定超高效液相色谱-串联质谱法Determinationadditionofolaquindoxandmequindoxintraditionalchineseveterinarydrug—highperformanceliqudchromatography-tandemmassspectrometry2020-07-09发布2020-08-09实施山东省市场监督管理局发布DB37/T4051—2020I目次前言................................................................................II1范围..............................................................................12规范性引用文件....................................................................13原理..............................................................................14试剂或材料........................................................................15仪器设备..........................................................................26测定步骤..........................................................................26.1提取..........................................................................26.2标准曲线的制备................................................................26.3仪器参考条件..................................................................26.4测定..........................................................................37数据处理..........................................................................38检测方法的精密度..................................................................4附录A（资料性附录）喹乙醇、乙酰甲喹特征离子质量色谱图..............................5DB37/T4051—2020II前言本标准按照GB/T1.1－2009给出的规则起草。本标准由山东省畜牧兽医局提出并组织实施。本标准由山东省畜牧业专业标准化技术委员会归口。本标准起草单位：山东省兽药质量检验所。本标准主要起草人：章安源、牛华星、张传津、李有志、陈玲、刘霄飞、陆庆泉、陈志强、魏秀丽、张志民、杨修镇。DB37/T4051—20201中兽药散剂中添加喹乙醇、乙酰甲喹的测定超高效液相色谱-串联质谱法1范围本标准规定了中兽药散剂中喹乙醇、乙酰甲喹的超高液相色谱-串联质谱测定方法。本标准适用于中兽药散剂中喹乙醇、乙酰甲喹的测定。本方法喹乙醇...
