Designation:D3264–97StandardSpecificationforIndustrialGradeAniline1ThisstandardisissuedunderthefixeddesignationD3264;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscriptepsilon(e)indicatesaneditorialchangesincethelastrevisionorreapproval.1.Scope1.1Thisspecificationcoversindustrialgradeaniline.1.2Thefollowingappliestoallspecifiedlimitsinthisspecification:forpurposesofdeterminingconformancewiththisspecification,anobservedvalueoracalculatedvalueshallberoundedoff“tothenearestunit”inthelastright-handdigitusedinexpressingthespecificationlimitinaccordancewiththerounding-offmethodofPracticeE29.1.3ConsultcurrentOSHAregulations,suppliers’MaterialSafetyDataSheets,andlocalregulationsforallmaterialsusedinthisspecification.NOTE1—Thepropertiesincludedinthisspecificationarethosere-quiredtocharacterizetheabovematerial.Ifadditionsaredeemednecessary,thesewillbeaddedwhentheirinclusionbecomesdesirableandthenecessarymethodsbecomeavailable.2.ReferencedDocuments2.1ASTMStandards:D1078TestMethodforDistillationRangeofVolatileOrganicLiquids2D1209TestMethodforColorofClearLiquids(Platinum-CobaltScale)2D1493TestMethodforSolidificationPointofIndustrialOrganicChemicals2D3436PracticeforSamplingandHandlingAniline2D3505TestMethodforDensityorRelativeDensityofPureLiquidChemicals2D4589TestMethodforNitrobenzeneinAniline2E29PracticeforUsingSignificantDigitinTestDatatoDetermineConformancewithSpecifications3E203TestMethodforWaterUsingKarlFischerReagent42.2OtherDocument:OSHARegulations,29CFR,paragraphs1910.1000and1920.120053.Properties3.1Industrialgradeanilineshallconformtothefollowingrequirements:PropertySpecificationASTMTestMethodNitrobenzene,max,weight%0.0002D4589Water,max,weight%0.05E203AppearanceAColor,max,PT/Coscale100D1209Distillationrange,includingthetemperature,184.2°C,at101.3kPa(760mmHg)pressure,max°CTotal1.0D107895%(2.0mLto97.0mL)0.5Relativedensity,20/4°C...
